Soxhlet extraction from leaves

VC2.4.2.1
Soxhlet extraction from leaves
Soxhlet extraction from leaves

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Description

When low solubility or insoluble solids are to be extracted, then a Soxhlet extraction is carried out as in experiment C2.4.2.1. In this case the vapourised solvent condenses on a chiller and drips onto the extraction material in a filter sleeve. It collects in the extraction space, draws the extract out of the extraction material, and is automatically drawn into the flask. From there the solvent evaporates once again (without extract).

Components of equipment sets

1 665453  4  Extraction unit after Soxhlet LD
1 665422  8  Counter-flow coller after Dimroth LD
1 664301  4  Round-bottom flask, 250 ml, ST 19/26 LD
1 665391  4  Joint clip, plastic, ST 19/26 LD
1 665392  4  Joint clip plastic, ST 29/32 LD
1 6666523  4  Heating Mantle, 250 ml, adjustable LD
1 30076  8  Laborboy 16 cm x 13 cm LD
1 30001  4  Stand base, V-shaped, large LD
1 30043  8  Stand rod, 75 cm, 12 mm diam. LD
2 666555  4  Universal clamp 0...80 mm LD
2 30109  4  Bosshead S LD
2 667193  4  PVC tubing, 7 mm diam., 1 m LD
2 604460  4  Hose clamp, 8...12 mm LD
1 661050  4  Extraction thimbles, 80 x 26 mm diam., 25 pieces LD
1 667027  4  Tweezers, blunt, 130 mm LD
1 602954  4  Measuring cylinder, Boro 3.3, 250 ml, glass base LD
1 661167  4  Narrow-neck bottle, amber glass, 250 ml LD
1 665005  4  Funnel, Boro 3.3, 100 mm diam. LD
1 6719720  4  Ethanol, denaturated, 1 l LD
GHS02GHS07 Danger H225 H319
1 6610821 Stopcock grease LD
1 661091  4  Boiling stones 100 g LD
1 additionally required:
leaves, dry, fine powder

Experiment Instructions

PDF (Experiment description) PDF (Experiment description) C2.4.2.1 Soxhlet extraction from leaves
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